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Successful scale-up means that larger scale operations are fully anticipated and understood. Usually, the performance will be poorer than witnessed on a smaller scale. Scale-up must address several interdependent, ow-sensitive physical processes occurring simultaneously. These are dispersion, dispersion kinetics, coalescence, and drop suspension, as mentioned previously. Scale-up is system dependent. For example, the scale-up of a dilute, neutraldensity, noncoalescing system is a matter of balancing shear with dispersion time. However, the scale-up of a concentrated coalescing liquid liquid system is much more complex. For this case, scale differences in uid ow in the vessels result in different proportions of the vessel causing coalescence and dispersion. The small vessel tends to be dominated by dispersion, and the large one, by coalescence. This is due to coalescence being promoted by gentle shear leading to soft, longduration collisions, while dispersion requires unsteady intense shear. In turbulent ow, rates of drop deformation, collision, and lm drainage are governed by the small scale turbulence structure, which is somewhat insensitive to tank size. However, the amount of time that drops spend in the high-shear and quiescent regions depends on mean circulation time, governed by impeller pumping rate and macroscale turbulence phenomena. These are strongly in uenced by tank size, so the balance of these rates is not readily scaled. These widely different conditions exist in all stirred vessels. In light of these complexities, scaling up liquid liquid systems using rules such as constant tip speed or power per volume can lead to failures. Scale-up practices are discussed in Section 12-8.

(via the runSample service) As part of the contract for the runSample service, the AA informs the ADA of the results of the experiment and these are logged along with the appropriate experimental settings (using the recordAnalysis service) Upon receipt of these results, the ADA informs the INA about them The INA then disseminates the results (via the notifyInterestedParties service) to scientists who have registered an interest in results of that kind (achieved via the registerInterest service) When interesting results are received, the SA alerts the scientist (via the resultAlert service) The scientist then examines the results and decides that they are of interest and that further analysis is needed The scientist then instructs the SA to make a booking on the High Resolution Analyser (via the bookSlot service).

4 ; :

Alkylation of isoprene at the methyl group was achieved through the reaction of the corresponding metal derivative (tert-BuOK-lithium tetramethylpiperidine, THF) with I-bromoheptane (60% yield) 57 Regioselective monoalkylation of isopropenylacetylene can be performed in high yields through the dilithium derivative: 258

When the booking is made, the HRAA volunteers information to the scientist about the con gurations of similar experiments that have previously been run (via the suggestRelatedConfigurations service) Using this information, the scientist sets the appropriate con gurations (via the configureParameters service) At the appropriate time, the experiment is started (via the runAnalysis service) As part of the contract for this service, the experiment is videoed (via the videoAnalysis service), monitoring information is sent to the technician (via the monitorAnalysis service) and a report is prepared and sent to the SA (via the reportResults service) In preparing this report, the HRAA interacts with the ERA to discover if related experiments and results have already been undertaken (achieved via the findSimilarExperiments service) The scientist is alerted to the report by the SA (via the reportAlert service).

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The scientist decides the results may be interesting and decides to replay some of the key segments of the video (via the replayExperiment service) The scientist decides the results are indeed interesting and so asks for relevant publications and details of scientists who have published any material on this topic This latter activity is likely to be provided through an external marketplace that provides this service for the wider community (see Table 173) In such a marketplace, there may be multiple Paper Repository Agents.

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